Course detail

Analytical Chemistry I

FCH-BCA_ANC1Acad. year: 2009/2010

The structure of contemporaneous analytical chemistry. Principles of analytical metrology. Analytical aspects of chemical equilibrium (thermodynamics and kinetics). Explanation of protolytic, complexation, redox, catalytic and inductive reactions. Principles of inorganic qualitative analysis, analytical selectivity and limits. Analytical signal and its qualitative and quantitative evaluation. Problems of sampling. Chemical and physical analytical methods. Gravimetric analysis and its present significance. Principles of solution volumetry. Theory of titration curves and titration characteristics and titration errors. Estimation and evaluation of titration equivalent points. The principles of buffering- acidobasic, redox, ligand and cation buffers. Examples of acidobasic, redox, precipitation and complexometric titrations.Lliquid-liquid extraction, analytical use of ion exchangers.

Language of instruction

Czech

Number of ECTS credits

5

Mode of study

Not applicable.

Guarantor

prof. Ing. Josef Čáslavský, CSc.

Department

Institute of Chemistry and Technology of Environmental Protection (ÚCHTOŽP)

Learning outcomes of the course unit

Relationship between chemical reactivity and analytical behavior of elements and compounds.
Principle of reactivity of ions and methods of standardization of analytical procedures.
Numerical solution of simple analytical problems.

Prerequisites

Basic and inorganic chemistry.

Co-requisites

Not applicable.

Planned learning activities and teaching methods

Teaching methods depend on the type of course unit as specified in the article 7 of BUT Rules for Studies and Examinations.

Assesment methods and criteria linked to learning outcomes

Course-unit credit in calculation lessons - test with successful results.
Requirement for the examination - course-unit credit in calculation lessons, in laboratory lessons and passing General, Inorganic and Physical chemistry examinations.
The examination consists of both written and oral parts.
Writtne part of the examination consists of questions from 3 topics: Theory (1 question ), Qualitative analysis (2 questions - cations and anions), Quantitative analysis (1 question). Mark F obtained in any of the topics = F from the whole written part.
Classification according to knowledge of theory and practical aspects of analytical chemistry.

Course curriculum

Introduction
Acid-base reactions
Complexometric reactions
Precipitation reactions
Redox reactions
Principles of kinetics of analytical reactions, catalytic reactions
Principles of identification of inorganic ions
Gravimetric analysis
Titrations
Acid-base titrations
Redox titrations
Precipitation titrations
Complexometric titrations

Work placements

Not applicable.

Aims

The aim of the course is to survey the following items: analytical application of chemical reactivity, principles of chemical qualitative analysis and methods of chemical quantitative analysis. It also shows the position of analytical chemistry in the system of chemical sciences.

Specification of controlled education, way of implementation and compensation for absences

Written test in the course of semester.
Consultations for students in distant form.
Consultations for students.

Recommended optional programme components

Not applicable.

Prerequisites and corequisites

Not applicable.

Basic literature

Bartoš M., Šrámková J., Staněk V., Renger F., Kalous J.: Analytická chemie I. Universita Pardubice, 2004. (CS)
Sommer L.: Základy analytické chemie I. Skriptum FCH VUT, VUTIUM Brno 1998 (CS)

Recommended reading

Jančářová I., Jančář L.: Základní chemické výpočty. MZLU, Brno 2002. (CS)
Šůcha L., Kotrlý S.: Teoretické základy analytické chemie, SNTL / ALFA, Praha 1971. (CS)
Vláčil F. a kol.: Příklady z chemické a instrumentální analýzy. SNTL Praha, 1978; Informatorium Praha, 1991. (CS)

Classification of course in study plans

  • Programme BPCP_CHCHT Bachelor's

    branch BPCO_CHM , 2 year of study, winter semester, compulsory
    branch BPCO_CHTOZP , 2 year of study, winter semester, compulsory
    branch BPCO_SCH , 2 year of study, winter semester, compulsory

  • Programme BPCP_CHTP Bachelor's

    branch BPCO_BT , 2 year of study, winter semester, compulsory
    branch BPCO_CHP , 2 year of study, winter semester, compulsory

  • Programme BKCP_CHCHT Bachelor's

    branch BKCO_CHTOZP , 2 year of study, winter semester, compulsory
    branch BKCO_CHM , 2 year of study, winter semester, compulsory
    branch BKCO_SCH , 2 year of study, winter semester, compulsory

  • Programme BKCP_CHTP Bachelor's

    branch BKCO_BT , 2 year of study, winter semester, compulsory
    branch BKCO_PCH , 2 year of study, winter semester, compulsory

  • Programme CKCP_CZV lifelong learning

    branch CKCO_CZV , 1 year of study, winter semester, compulsory

Type of course unit

 

Lecture

26 hod., optionally

Teacher / Lecturer

prof. Ing. Josef Čáslavský, CSc.

Exercise

26 hod., compulsory

Teacher / Lecturer

prof. Ing. Josef Čáslavský, CSc.
Ing. Ludmila Mravcová, Ph.D.
Mgr. Helena Doležalová Weissmannová, Ph.D.

Guided consultation in combined form of studies

52 hod., optionally

Teacher / Lecturer

prof. Ing. Josef Čáslavský, CSc.