Course detail
Analytical Chemistry I
FCH-BAA_ANC1Acad. year: 2009/2010
The structure of contemporaneous analytical chemistry. Principles of analytical metrology. Analytical aspects of chemical equilibrium (thermodynamics and kinetics). Explanation of protolytic, complexation, precipitation, redox, catalytic and inductive reactions. Organic analytical reagents Principles of inorganic qualitative analysis, group and selective analytical reactions, analytical selectivity and limits. Analytical signal and its qualitative and quantitative evaluation. Problems of sampling. Chemical and physical analytical methods. Gravimetric analysis and its present significance. Processes during precipitate formation and contamination. Modern analytical balances and correct weighing.. Examples of gravimetric procedures. Gravimetric stoichiometry. Organic reagents in gravimetry. Precipitation in homogeneous solution. Errors in gravimetry. Principles of solution volumetry. Theory of titration curves, titration characteristics and titration errors. Estimation and evaluation of titration equivalent points. Chemical indicators The principles of buffering acidobasic, redox, ligand and cation buffers. Examples of acidobasic, redox, precipitation and complexometric titrations. Acidimetry and alkalimetry. Titration of weak acids and bases. Boric acid, aminoacids, ammonium, ammonia, nitrogen in organic compounds, polyprotic acids. Titration of weak bases, carbonate, hydrogencarbonate. Theory and examples of iodometry, chromatometry, bromatometry and cerimetry. Precipitation titration. Argentometry with various indicators of the end-point, determination of sulphate. Titration on the basis of of complexes (chelates), cyanide, mercurimetry, EDTA titrations. Theory of titration curves and practical examples of chelometric titration. Metalochromic indicators.
Language of instruction
Number of ECTS credits
Mode of study
Guarantor
Offered to foreign students
Learning outcomes of the course unit
Gravimetric analysis and its contemporaneous significants.
Principles, theorie and practise of solution volumetry.
Numerical solution of simple analytical problems.
Prerequisites
Co-requisites
Planned learning activities and teaching methods
Assesment methods and criteria linked to learning outcomes
Examination - written and oral parts.
Course curriculum
Quantitative analysis on the basis of chemical reactions - gravimetry, volumetry
Work placements
Aims
Specification of controlled education, way of implementation and compensation for absences
Oral consultations in the extent of lectures.
Recommended optional programme components
Prerequisites and corequisites
Basic literature
Recommended reading
L.Sommer: CD-ROM in Analytical Chemistry I (EN)
Skoog, West, Holler, Crouch, Analytical chemistry. An Itroduction, Thomson learning, USA,2000 (EN)
Classification of course in study plans
- Programme BPCP_CHCHT Bachelor's
branch BPCO_CHM , 2 year of study, winter semester, compulsory
branch BPCO_CHTOZP , 2 year of study, winter semester, compulsory
branch BPCO_SCH , 2 year of study, winter semester, compulsory - Programme BPCP_CHTP Bachelor's
branch BPCO_BT , 2 year of study, winter semester, compulsory
branch BPCO_CHP , 2 year of study, winter semester, compulsory - Programme BKCP_CHCHT Bachelor's
branch BKCO_CHTOZP , 2 year of study, winter semester, compulsory
branch BKCO_CHM , 2 year of study, winter semester, compulsory
branch BKCO_SCH , 2 year of study, winter semester, compulsory - Programme BKCP_CHTP Bachelor's
branch BKCO_BT , 2 year of study, winter semester, compulsory
branch BKCO_PCH , 2 year of study, winter semester, compulsory - Programme NPCP_CHM_INT Master's
branch NPCO_CHM , 1 year of study, winter semester, elective
- Programme BPCP_CHCHT_INT Bachelor's
branch BPCO_CHTOZP , 1 year of study, winter semester, elective
branch BPCO_CHM , 1 year of study, winter semester, compulsory - Programme CKCP_CZV lifelong learning
branch CKCO_CZV , 1 year of study, winter semester, compulsory
Type of course unit
Seminar
Teacher / Lecturer
Guided consultation in combined form of studies
Teacher / Lecturer