Course detail

Methods of Instrumental Analysis

FCH-MC_MIAAcad. year: 2022/2023

Instrumental techniques for characterization of properties of colloids (particles size and charge, interactions, thermodynamic and transport properties) and surface (wetting, contact angle, atomic force microscopy), methods for analysis of colloidal and special materials (thermic, viscoelastic, electric and electro-optical properties, microscopy).

Language of instruction

Czech

Number of ECTS credits

Mode of study

Not applicable.

Guarantor

Ing. Michal Kalina, Ph.D.

Department

Institute of Physical and Applied Chemistry (ÚFSCH)

Learning outcomes of the course unit

Students attending the course will be able to describe the basic principles of selected methods of structural analysis and methods for characterisation of colloidal systems and materials used in modern chemistry and chemical technology and for surface analysis. Student will be able to select appropriate method for given analysis, its basic settings and make data processing.

Prerequisites

physical chemistry, analytical chemistry

Co-requisites

Not applicable.

Planned learning activities and teaching methods

The course uses teaching methods in form of Lecture - 2 teaching hours per week. The e-learning system (LMS Moodle) is available for teachers and students.

Assesment methods and criteria linked to learning outcomes

Written and oral exam.

Course curriculum

Characterization of colloidal systems and surfaces
1. Size distribution of particles and macromolecules (light scattering, SEC)
2. Charge (zeta potential) and wetting of surface, contact angle
3. Atomic force microscopy (AFM)
4. Microcalorimetry (DSC, ITC, IC)
5. Transport properties (sorption and diffusion techniques
Materials analysis
6. Thermochemical analysis (DSC, TG)
7. Rheology and viscometry
8. Electric and electro-optical properties
9. Microscopy (optical and electron)
10.-13. Practical excursions, measurement and data processing

Work placements

Not applicable.

Aims

Describe the principles of selected techniques of structural analysis, methods used for characterisation of colloidal systems and materials generally used in modern chemistry, chemical technology and in surface analysis. Describe the ways how to select appropriate instrumental technique, settings the measurement parameters and data processing.

Specification of controlled education, way of implementation and compensation for absences

none

Recommended optional programme components

Not applicable.

Prerequisites and corequisites

Not applicable.

Basic literature

Bartovská, L.; Šišková, M.: Fyzikální chemie povrchů a koloidních soustav, Praha: VŠCHT, 2005. (CS)
Klouda, P.: Moderní analytické metody, Ostrava: Nakladatelství Pavel Klouda, 1996.
Skoog, D. A, Holler, J.: Principles of instrumental analysis, Cengage Learning, 2017. (EN)
Sommer, L.: Teoretické základy analytické chemie I, II, III, VUTIUM, 1995, 1998, 2000. (CS)

Type of course unit

Lecture

26 hod., optionally

Teacher / Lecturer

doc. Ing. Petr Dzik, Ph.D.
doc. Ing. Ota Salyk, CSc.
prof. Ing. Oldřich Zmeškal, CSc.
Ing. Michal Kalina, Ph.D.
Ing. Jitka Krouská, Ph.D.
doc. Ing. Petr Sedláček, Ph.D.
Ing. Jiří Smilek, Ph.D.

Guided consultation in combined form of studies

26 hod., optionally

Teacher / Lecturer

Ing. Michal Kalina, Ph.D.

Elearning

eLearning: currently opened course