Course detail
Laboratory Classes in Instrumental Analysis
FCH-MC_PIAAcad. year: 2021/2022
Methods of instrumental analysis - realization of given tasks.
Language of instruction
Czech
Number of ECTS credits
3
Mode of study
Not applicable.
Guarantor
Learning outcomes of the course unit
Practice in chosen experimental methods of instrumental and structural analysis
Prerequisites
basic knowledge of analytical and instrumental chemistry
Co-requisites
Not applicable.
Planned learning activities and teaching methods
The course uses teaching methods in form of Laboratory exercise - 3 teaching hours per week. The e-learning system (LMS Moodle) is available to teachers and students.
Assesment methods and criteria linked to learning outcomes
Conditions for awarding the course-unit credit is realization of selected tasks and properly kept laboratory notebook. Details are described in e-learning. Requirement for credits are agreement of teachers of the individual tasks - signatures in laboratory notebook.
Course curriculum
Methods of instrumental analysis - realization of given tasks.
0. Introduction
1. Lyophilization and morphologic characterization by SEM
2. Vibrational Spectroscopy I - sampling and measuring techniques
3. Densitometry and viscometry
4. Utilization of microcalorimetry in study of binding and phase equilibriums
5. Fluorescence spectroscopy
6. AFM - atomic force microscopy
7. HRUS - high resolution ultrasound spectroscopy
8. Vibrational Spectroscopy II - qualitative and quantitative analysis
9. Potentiometric and conductometric titrations
10. Methods of anorganic and organic elemental analysis (ICP-OES and EA)
0. Introduction
1. Lyophilization and morphologic characterization by SEM
2. Vibrational Spectroscopy I - sampling and measuring techniques
3. Densitometry and viscometry
4. Utilization of microcalorimetry in study of binding and phase equilibriums
5. Fluorescence spectroscopy
6. AFM - atomic force microscopy
7. HRUS - high resolution ultrasound spectroscopy
8. Vibrational Spectroscopy II - qualitative and quantitative analysis
9. Potentiometric and conductometric titrations
10. Methods of anorganic and organic elemental analysis (ICP-OES and EA)
Work placements
Not applicable.
Aims
The aim of the subject is to acquire measuring technique and to acquaint students with practical problems of chosen methods of instrumental analysis.
Specification of controlled education, way of implementation and compensation for absences
Student attends given tasks in agreement with their teachers, which is checked on the basis of the laboratory date-book by garant.
LABORATORY DATE-BOOK
Notes in laboratory date-book are destined for archivation of course and results of laboratory activities. Following details should be included in date-book:
date of record (date of laboratory activity),
name of laboratory activity,
reason of laboratory activity,
description of operating procedure,
all actual data (weights, concentrations, temperatures...),
obtained results (in written or electronic form).
other notes or problems in measurements
number of page
LABORATORY DATE-BOOK
Notes in laboratory date-book are destined for archivation of course and results of laboratory activities. Following details should be included in date-book:
date of record (date of laboratory activity),
name of laboratory activity,
reason of laboratory activity,
description of operating procedure,
all actual data (weights, concentrations, temperatures...),
obtained results (in written or electronic form).
other notes or problems in measurements
number of page
Recommended optional programme components
Not applicable.
Prerequisites and corequisites
Not applicable.
Basic literature
Čůta, K. a kol.. Instrumentální analýza. SNTL, Praha 1986. (CS)
dle zadání vedoucího vybraného úkolu (CS)
dle zadání vedoucího vybraného úkolu (CS)
Recommended reading
Not applicable.
Elearning
eLearning: currently opened course
Classification of course in study plans
- Programme NPCP_CHCHTE Master's 1 year of study, winter semester, compulsory
- Programme NKCP_CHCHTE Master's 1 year of study, winter semester, compulsory
Type of course unit
Guided consultation in combined form of studies
26 hod., optionally
Teacher / Lecturer
Laboratory exercise
39 hod., compulsory
Teacher / Lecturer
prof. Ing. Martina Klučáková, Ph.D.
doc. Ing. Zdenka Kozáková, Ph.D.
doc. Ing. Petr Dzik, Ph.D.
Ing. Jitka Krouská, Ph.D.
doc. Ing. Petr Sedláček, Ph.D.
doc. Ing. Filip Mravec, Ph.D.
Ing. Jiří Smilek, Ph.D.
doc. Ing. Ota Salyk, CSc.
prof. RNDr. František Krčma, Ph.D.
Ing. Michal Kalina, Ph.D.
prof. Ing. Michal Veselý, CSc.
prof. Ing. Miloslav Pekař, CSc.
doc. Ing. Vojtěch Enev, Ph.D.
doc. Ing. Zdenka Kozáková, Ph.D.
doc. Ing. Petr Dzik, Ph.D.
Ing. Jitka Krouská, Ph.D.
doc. Ing. Petr Sedláček, Ph.D.
doc. Ing. Filip Mravec, Ph.D.
Ing. Jiří Smilek, Ph.D.
doc. Ing. Ota Salyk, CSc.
prof. RNDr. František Krčma, Ph.D.
Ing. Michal Kalina, Ph.D.
prof. Ing. Michal Veselý, CSc.
prof. Ing. Miloslav Pekař, CSc.
doc. Ing. Vojtěch Enev, Ph.D.
Elearning
eLearning: currently opened course