Course detail
Laboratory Classes in Instrumental and Structure Analysis - MS
FCH-MCA_ISA_MAcad. year: 2009/2010
Students will introduce basic methods for research and evaluation of supramolecular structure and thermo-mechanical properties of polymer materials. Used are microscopy and spectroscopy methods and methods of thermo-mechanical analysis. The stress is laid on the accurate evaluation and interpretation of the obtained data and an examination of particular method availability for the tested material.
Language of instruction
Number of ECTS credits
Mode of study
Guarantor
Department
Learning outcomes of the course unit
Prerequisites
Co-requisites
Planned learning activities and teaching methods
Assesment methods and criteria linked to learning outcomes
- attendance at all exercises,
- handover of all laboratory reports in time and in a required quality,
- completion of a credit test - minimum score is 50%
Course curriculum
2) Theory: Polymer structure, Optical (Light) Microscopy (OM)
Task: Structure of polypropylene (PP)
3) Theory: Microscopic methods
a. Laser Scanning Confocal Microscopy (LSCM),
b. Scanning and Transmission Electron Microscopy (SEM and TEM),
c. Atomic Force Microscopy (AFM) and
d. Scanning Tunneling Microscopy (STM).
Task: 3D image of polypropylene structure
4) Theory: Thermogravimetry (TA)
Task: Decomposition of ethylenvynilacetate (EVA) copolymer, filler content determination
5) Theory: Differential Scanning Microscopy (DSC),
Stabilizer effectiveness determination - Oxidative Induction Time/Temperature (OIT) determination
Task: Polymer type determination, calculation of crystalinity
6) Theory: X-ray Diffraction (XRD)
Task: Amorphous and semicrystaline polymers evaluation, qualitative analysis of mineral mixture
7) Theory: Infrared Spectroscopy (IR)
Task: Interpretation of IR spectra, Identification of unknown sample
8) Theory: Dynamic-Mechanical Analysis (DMA)
Task: Interpretation of DMA records
9) Theory: Wetting of solids, Liquid surface tension, Surface free energy
Task: Interpretation of data from dynamic wetting of PET roll of film with a diameter of 20 m
10-11) Package teaching of subject "Preparation and Control of Projects"
12) Presentation concerning ISA = requirement for subject "Preparation and Control of Projects"
13) Credit test
Work placements
Aims
Specification of controlled education, way of implementation and compensation for absences
The examination of basic knowledge relating to the particular project is done at the beginning of each exercise (oral or in writing).
Laboratory reports are required till 7 days after the last exercise at the latest.
Recommended optional programme components
Prerequisites and corequisites
Basic literature
Recommended reading
Classification of course in study plans