Course detail

Instrumental and structure analysis

FCH-MC_ISAAcad. year: 2009/2010

Fundamentals, instrumentation and usage of methods of chemical, physical and structure analysis. Separation methods: chromatography methods-gas chromatography, liquid chromatography, supercritical fluid chromatography; electrophoresis, isotachophoresis. Electroanalysis: special voltammetry.Thermal analysis: thermogravimetry, differential thermal analysis, differential scanning calorimetry. Atomic spectrometry: Atomic emission spectrometry, atomic absorption spectrometry, atomic fluorescence spectrometry. X-ray fluorescence spectrometry. Mass spectrometry organic and inorganic. Infrared and Raman spectroscopy. Nuclear magnetic resonance spectroscopy. Electron spin resonance spectroscopy. Moessbauer spectrometry. Photoelectron spectroscopy (ESCA, Auger spectroscopy). Microbeam and surface analysis: Photon probe techniques, electron probe techniques, ion probe techniques(SEM, TEM, EPXMA,SIMS,FIM,STM, AFM). X-ray diffraction. Laser in analytical chemistry. Hyphenated techniques.

Language of instruction

Czech

Number of ECTS credits

Mode of study

Not applicable.

Guarantor

prof. Ing. Josef Čáslavský, CSc.

Department

Institute of Chemistry and Technology of Environmental Protection (ÚCHTOŽP)

Learning outcomes of the course unit

Fundamental principles and theoretical knowledge of chosen analytical method and instrumentation and their application in industry and environmental regulation. New instruments and strategies for new technologies.

Prerequisites

Basic knowladge of physics, general chemistry, physical chemistry, inorganic, organic, analytical chemistry and biochemistry.

Co-requisites

Not applicable.

Planned learning activities and teaching methods

Teaching methods depend on the type of course unit as specified in the article 7 of BUT Rules for Studies and Examinations.

Assesment methods and criteria linked to learning outcomes

Oral examination.

Course curriculum

Separation methods: chromatography methods-gas chromatography, liquid chromatography, supercritical fluid chromatography; electrophoresis, isotachophoresis.Thermal analysis: thermogravimetry, differential thermal analysis, differential scanning calorimetry. Atomic spectrometry: Atomic emission spectrometry, atomic absorption spectrometry, atomic fluorescence spectrometry. X-ray fluorescence spectrometry. Infrares spectometry. Mass spectrometry. Nuclear magnetic resonance spectroscopy. Electron spin resonance spectroscopy. Photoelectron spectroscopy (UPS,ESCA, Auger spectroscopy). Microbeam and surface analysis: Photon probe techniques, electron probe techniques, ion probe techniques,(SEM, TEM, EPXMA,SIMS,FIM,STM, AFM). X-ray diffraction. Laser in analytical chemistry. Hyphenated techniques.

Work placements

Not applicable.

Aims

The aim of the course is to acquire both survey and intensive knowledge of selected methods of instrumental analysis according to their use for the analysis of the composition and structure of real objects in industry and research..

Specification of controlled education, way of implementation and compensation for absences

none

Recommended optional programme components

Not applicable.

Prerequisites and corequisites

Not applicable.

Basic literature

Kellner R., Mermet J. M., Otto M., Widmer H. M.: Analytical Chemistry. Willey-VCH, Weinheim 1998. (EN)
Sommer L.: Teoretické základy analytické chemie I., II., III. VUT Brno, Brno 1995. (CS)

Type of course unit

Lecture

26 hod., optionally

Teacher / Lecturer

prof. Ing. Josef Čáslavský, CSc.