Course detail

Analytical Methods of Technical Praxis

FCH-BCO_AMPAcad. year: 2009/2010

Basic rules of analytical sampling. Procedures for sample treatments: Isolation of target analytes from sample matrix (extraction by gal, liquid, solid phase), clean-up techniques (destructive, non-destructive), methods of group separation. Instrumental analytical methods used in analytical praxis: UV-VIS spectrophotometry, separation methods (gas and liquid chromatography, electromigration techniques), mass spectrometry. Basic principles of interpretation of analytical results.

Language of instruction

Czech

Number of ECTS credits

Mode of study

Not applicable.

Guarantor

prof. Ing. Josef Čáslavský, CSc.

Department

Institute of Chemistry and Technology of Environmental Protection (ÚCHTOŽP)

Learning outcomes of the course unit

Information about methods and techniques applied for the environmental sampling, but mainly for the laboratory treatment and final analysis of the sample, and also about the interpretation of analytical results.

Prerequisites

Knowledge from courses Common and Inorganic Chemistry, Organic chemistry, Physical chemistry, Analytical chemistry I, Analytical Chemistry II

Co-requisites

Not applicable.

Planned learning activities and teaching methods

Teaching methods depend on the type of course unit as specified in the article 7 of BUT Rules for Studies and Examinations.

Assesment methods and criteria linked to learning outcomes

The evaluation of student's knowledge is based on oral examination.

Course curriculum

1. Introduction, importance of analytical chemistry in technical praxis
2. Basic principles of analytical sampling
3. Methods of target analytes isolation from sample matrix
4. Techniques of clean-up and group separation
5. UV-VIS Spectrophotometry, principle and applications
6. Gas chromatography - principle, instrumentation, application in technical praxis
7. Liquid chromatography - principle, instrumentation, application in technical praxis
8. Electromigration methods - principle, classification, instrumentation, application in technical praxis
9. Mass spectrometry - physica basics, principle, instrumentation, acquiring and interpretation of mass spectra, application for the analysis of inorganic and organic materials
10. Hyphenated techniques and their application in technical praxis
11. Basic rules of analytical results treatment and interpretation

Work placements

Not applicable.

Aims

The aim of the course is the introduction of methods and techniques frequently used in analytical praxis

Specification of controlled education, way of implementation and compensation for absences

Consultations within the range of lectures for the students of the distant form
Consultations for regular students
Using of the materials in electronic teaching support system Moodle

Recommended optional programme components

Not applicable.

Prerequisites and corequisites

Not applicable.

Basic literature

Klouda P.: Moderní analytické metody. 2. vyd. Ostrava: Nakladatelství Pavel Klouda, 2003 (CS)
Štulík, K. a. kol.: Analytické separační metody. 1. vyd. Praha: KU Praha, 2005 (CS)
Volka, K. a. kol.: Analytická chemie 2. 1. vyd. Praha: Vydavatelství VŠCHT, 1995 (CS)

Type of course unit

Lecture

26 hod., optionally

Teacher / Lecturer

prof. Ing. Josef Čáslavský, CSc.