Course detail

Laboratory Classes in Analytical Chemistry II

FCH-BAA_ANC2_PAcad. year: 2024/2025

Practical teaching of selected basic instrumental analytical methods: molecular spectrophotometry and fluorimetry, atomic absorption and emission spectrometry, separation techniques: liquid, gas and thin-layer chromatography, gel electrophoresis and XRF, SEM and NMR methods.

Language of instruction

English

Number of ECTS credits

Mode of study

Not applicable.

Guarantor

doc. Mgr. Renata Komendová, Ph.D.

Department

Institute of Chemistry and Technology of Environmental Protection (ÚCHTOŽP)

Offered to foreign students

The home faculty only

Entry knowledge

Laboratory Classes in Analytical chemistry I.

Rules for evaluation and completion of the course

Graded course-unit credit
Requirements:
- all laboratory tasks completed, results and reports in good quality
- course test (15-20 questions)
Final classification is based on average classification of individual tasks.
Classification:
100-90% A
89-80% B
79-70% C
69-60% D
59-50% E
49-0% F

Written entrance tests at the beginning of all exercises checking the students readiness for practical work.
Credit test at the course end.

Aims

The aim of the Analytical Chemistry Practice II is to teach students the basics and use of selected instrumental analytical methods, such as molecular spectrophotometry and fluorimetry, atomic absorption and emission spectrometry, separation techniques liquid, gas and thin-layer chromatography, gel electrophoresis and XRF, SEM and NMR methods.

Completing the course will increase the students' competences as follows:

1. They will be practically acquainted with selected analytical methods.

2. They will be able to practically apply individual determination procedures.

3. They will practice precise work in the analytical laboratory, preparation of standard solutions and correct principles of working with samples.

4. Students will be able to handle all necessary calculations and will be able to evaluate analytical results obtained by individual analyses.

Study aids

Not applicable.

Prerequisites and corequisites

Not applicable.

Basic literature

Z.Šimek et al.: Quantitative analysis (EN)

Type of course unit

Laboratory exercise

78 hod., compulsory

Teacher / Lecturer

Ing. Simona Jonášová
Ing. Jan Koplík, Ph.D.
Ing. Matěj Březina, Ph.D.
Ing. Marie Hamplová
Mgr. Jan Richtár, Ph.D.
Pavla Kleinová
Ing. Juraj Marcinko
Ing. Veronika Řezáčová, Ph.D.
Ing. Anna Amrichová

Syllabus

1. INTRODUCTION TO PRACTICAL CHEMISTRY, WORK SAFETY, METHODOLOGY OF WORK IN THE ANALYTICAL LABORATORY

2. SPECTROPHOTOMETRY I

3. SPECTROPHOTOMETRY II - MULTICOMPONENT ANALYSIS

4. FLUORIMETRY

5. GEL ELECTROPHORESIS + THIN LAYER CHROMATOGRAPHY

6. FLAME EMISSION SPECTROMETRY

7. LIQUID CHROMATOGRAPHY

8. GAS CHROMATOGRAPHY

9. INFRARED SPECTROMETRY

10. ATOMIC ABSORPTION SPECTROMETRY

11. NMR

12. XRF, SEM

13. CREDIT TEST

Elearning

eLearning: currently opened course