Course detail
Experimental and Analytical Techniques of Practical Organic Synthesis
FCH-DA_EAPAcad. year: 2022/2023
Basic concepts, techniques and glassware, recrystallization and melting point, distillation and boiling point, extraction, methods of chromatography, spectral methods, identification of organic compounds.
Language of instruction
English
Mode of study
Not applicable.
Guarantor
Department
Learning outcomes of the course unit
Not applicable.
Prerequisites
Not applicable.
Co-requisites
Not applicable.
Planned learning activities and teaching methods
Not applicable.
Assesment methods and criteria linked to learning outcomes
Not applicable.
Course curriculum
This course is overview of experimental science that is based on a well-established theoretical framework where the basic aspects are well established but at the same time are under constant development. Therefore, it is essential for students to develop a strong background in the laboratory and analytical skills.
Basic concepts, techniques and glassware, recrystallization and melting point, distillation and boiling point, extraction, methods of chromatography, spectral methods, identification of organic compounds.
1. Apparatuses for advanced organic synthesis
2. Microfiltration and its technics
3. Dry agents
4. Drying of organic solvents
5. Crystallization and crystallization technics
6. Microscale experiments
7+8. Separation technics
9. Vacuum distillation technics
10+13. NMR and interpretation
Basic concepts, techniques and glassware, recrystallization and melting point, distillation and boiling point, extraction, methods of chromatography, spectral methods, identification of organic compounds.
1. Apparatuses for advanced organic synthesis
2. Microfiltration and its technics
3. Dry agents
4. Drying of organic solvents
5. Crystallization and crystallization technics
6. Microscale experiments
7+8. Separation technics
9. Vacuum distillation technics
10+13. NMR and interpretation
Work placements
Not applicable.
Aims
The aim of subject is a detailed study of the advanced organic synthesis techniques and methods of chemical research. Modern organic synthesis prefers mini and micro scale experiments requiring special glass and equipment. Organic chemistry is closely connects to the condition of product composition identification and the possibility of separating the individual components of the mixture.
The course structure is designed so that after completing this discipline, students are well prepared for modern research trends in the field of organic synthesis and characterization of organic molecules.
The course structure is designed so that after completing this discipline, students are well prepared for modern research trends in the field of organic synthesis and characterization of organic molecules.
Specification of controlled education, way of implementation and compensation for absences
Not applicable.
Recommended optional programme components
Not applicable.
Prerequisites and corequisites
Not applicable.
Basic literature
Gilbert, J.C., Martin, S.F., Experimental Organic Chemistry, Cengage Learning (EN)
WYATT, P., WARREN S.: Organicsynthesis, Strategy and Control, John Wiley&Sons Ltd. 2007 (EN)
WYATT, P., WARREN S.: Organicsynthesis, Strategy and Control, John Wiley&Sons Ltd. 2007 (EN)
Recommended reading
Not applicable.
Classification of course in study plans
- Programme DPAP_CHM_4_N Doctoral 1 year of study, winter semester, compulsory-optional
- Programme DKAP_CHM_4_N Doctoral 1 year of study, winter semester, compulsory-optional