Course detail

Laboratory Classes in Laboratory Technics I

FCH-BC_ACH1_PAcad. year: 2022/2023

Laboratory code and safety measures, basic laboratory work - weighing, measuring volumes of liquids, filtration, heating, annealing, cooling, dehydrating, distillation, crystallization, decantation, sublimation, extraction, determination of physical variables - refracting index, melting point, density, pH. Simple tasks - fraction crystallization, preparation of the solutions with accurate concentrations, distillation of salt acid, separation of a mixture by precipitation, gas preparation.

Language of instruction

Czech

Number of ECTS credits

Mode of study

Not applicable.

Guarantor

RNDr. Ivana Pilátová, CSc.

Department

Institute of Materials Science (ÚCHM)

Learning outcomes of the course unit

Obtaining skills and a practical knowledge of basic operations that are used in the chemical laboratory.

Prerequisites

Successful graduation of Legislation in Chemistry I and Basics of Laboratory Technique.
Knowledge of secondary school chemistry and basic mathematics.

Co-requisites

Not applicable.

Planned learning activities and teaching methods

The course uses teaching methods in form of Laboratory exercise - 4 teaching hours per week. The e-learning system (LMS Moodle) is available to teachers and students.

Assesment methods and criteria linked to learning outcomes

The laboratory notebook (control of preparation), report sheets, tests, style of the work, course-unit credit test.
Evaluation of the test: excellent [100%-90%], very good [89%-80%], good [79%-70%], satisfactory [69%-60%], sufficient [59%-50%], failed [49%-0%]
The average from the evalution of the report sheets, of the tests, of the final test and style of the work is the final evalution of the course.

Course curriculum

1. Introduction. Laboratory safety and guidelines, laboratory notes. Laboratory equipment.
2. Measuring volumes of liquids, volumetric glass. Filtration - gravity filtration. Weighing.
3. Temperature measurement. Heating. Cooling.
4. Filtration - vacuum filtration. Saturated solution, solubility curve. Evaporation,
crystallization - types. Drying.
5. Filtration (Büchner funnel), decanting, dehydrating. Determination of melting point. Annealing.
6. Gas preparation in the laboratory. Sublimation.
7. Extraction. Determination of index of refraction. Determination of density. Weighing.
8. Preparation of solutions with accurate concentrations. Titration - byrettes, pH measuring.
9. Distillation of hydrochloric acid.
10. Fraction crystallization of mixture chromium(III) oxide,borax and sodium chloride.
11. Separation of a mixture by precipitation.
12. Compensation for illness, for holiday.
13. Course-unit credit test.

Work placements

Not applicable.

Aims

The target of the course is an acquisition of laboratory knowledge of the starting students - chemists.

Specification of controlled education, way of implementation and compensation for absences

The attendance is compulsory. In the case of illness confirmed with a doctor is substitution in other students group possible.

Recommended optional programme components

Not applicable.

Prerequisites and corequisites

Not applicable.

Basic literature

B.Kábelová a kol.: Laboratorní technika II, Vutium, Brno 1999, ISBN 80-214-1450-2 (CS)

Type of course unit

Laboratory exercise

52 hod., compulsory

Teacher / Lecturer

doc. Ing. František Šoukal, Ph.D.
Ing. Jan Hajzler
Ing. Martin Buchtík, Ph.D.
Ing. Matěj Březina, Ph.D.
Ing. Jan Koplík, Ph.D.
Ing. Martin Sedlačík
Ing. Petr Poláček, Ph.D.
Eva Kocmanová
RNDr. Ivana Pilátová, CSc.
Ing. Eva Bartoníčková, Ph.D.
Ing. Vlastimil Bílek, Ph.D.
Ing. Radoslav Novotný, Ph.D.
Ing. Tomáš Plichta, Ph.D.
Ing. David Markusík
Ing. Luboš Bocian
Ing. Tomáš Horák
Ing. Jakub Palovčík

Elearning

eLearning: currently opened course