Course detail
Basics of Laboratory Technique
FCH-BA_ZLTAcad. year: 2022/2023
Theoretical knowledges of laboratory equipment which is necessary for practicePraktikum z anorganické chemie I a Praktikum z anorganické chemie II.
Laboratory safety, first aid and disposal of chemical wastes. Laboratory equipment, basic laboratory operations, such as working with glass, weighing, measuring volumes of liquids and gases, heating and cooling, annealing, dissolution and dilution, separation of components of heterogeneous mixtures (such as decantation, filtration), separating components of homogeneous mixtures (eg. crystallization, distillation), further separation and purification techniques (eg, drying, extraction, sublimation, recrystallization), measurement of physical quantities (melting point, refractive index, density, pH).
Language of instruction
Number of ECTS credits
Mode of study
Guarantor
Department
Offered to foreign students
Learning outcomes of the course unit
Prerequisites
Co-requisites
Planned learning activities and teaching methods
Assesment methods and criteria linked to learning outcomes
Course curriculum
Basic laboratory equipment (lab equipment, glass, porcelain).
Working with glass. Working with scales. Volume measuring of liquids and gases. Approximate measuring volumes of liquids. Working with dispenser and automatic pipette. Principles of work with a standard glass (graduated cylinders, volumetric flasks, pipettes, burettes). Working with automatic burette.
Heating and cooling. Direct heating, gas and alcohol burners. Electric heat source. Indirect heating (liquid, steam, air and other bath). Annealing. Cooling (coolant, cooling media).
Separation of components of heterogeneous mixtures (decantation, filtration).The methods of filtration. Separation of the components of homogenous mixtures (crystallization, distillation). Types of crystallization. Distillation (simple distillation, fractional distillation, rectification, steam distillation, distillation under reduced pressure).
Further separation and purification techniques (drying, extraction, sublimation and recrystallization). Measurement of physical quantities (melting point, refractive index, density, pH).
Work placements
Aims
Specification of controlled education, way of implementation and compensation for absences
Students elaborate final test on elearning in the end of the semester.
Recommended optional programme components
Prerequisites and corequisites
Basic literature
Recommended reading
Elearning
Classification of course in study plans
- Programme BPCP_CHCHT Bachelor's
branch BPCO_SCH , 1 year of study, winter semester, compulsory
branch BPCO_CHMN , 1 year of study, winter semester, compulsory
branch BPCO_CHM , 1 year of study, winter semester, compulsory
branch BPCO_CHTOZP , 1 year of study, winter semester, compulsory - Programme BKCP_CHCHT Bachelor's
branch BKCO_CHM , 1 year of study, winter semester, compulsory
branch BKCO_CHTOZP , 1 year of study, winter semester, compulsory
branch BKCO_SCH , 1 year of study, winter semester, compulsory - Programme BPCP_CHTP Bachelor's
branch BPCO_CHP , 1 year of study, winter semester, compulsory
branch BPCO_BT , 1 year of study, winter semester, compulsory - Programme BKCP_CHTP Bachelor's
branch BKCO_PCH , 1 year of study, winter semester, compulsory
branch BKCO_BT , 1 year of study, winter semester, compulsory - Programme BKCP_AAEFCH Bachelor's 1 year of study, winter semester, compulsory
- Programme BPCP_AAEFCH Bachelor's 1 year of study, winter semester, compulsory
- Programme BKCP_CHCHTE Bachelor's 1 year of study, winter semester, compulsory
- Programme BPCP_CHCHTE Bachelor's 1 year of study, winter semester, compulsory
- Programme BKCP_CHTM Bachelor's 1 year of study, winter semester, compulsory
- Programme BPCP_CHTM Bachelor's 1 year of study, winter semester, compulsory
- Programme BPCP_CHTOZP Bachelor's 1 year of study, winter semester, compulsory
- Programme BKCP_CHTOZP Bachelor's 1 year of study, winter semester, compulsory
- Programme BPCP_CHTPO Bachelor's
specialization CHPL , 1 year of study, winter semester, compulsory
specialization PCH , 1 year of study, winter semester, compulsory
specialization BT , 1 year of study, winter semester, compulsory - Programme BKCP_CHTPO Bachelor's
specialization PCH , 1 year of study, winter semester, compulsory
specialization BT , 1 year of study, winter semester, compulsory
specialization CHPL , 1 year of study, winter semester, compulsory - Programme BPCP_CHMA Bachelor's 1 year of study, winter semester, compulsory
- Programme NPAP_ENVI Master's 1 year of study, winter semester, compulsory
Type of course unit
Elearning