Course detail
Experimentální a analytické techniky praktické organické syntézy
FCH-DC_EAPAcad. year: 2022/2023
Basic concepts, techniques and glassware, recrystallization and melting point, distillation and boiling point, extraction, methods of chromatography, spectral methods, identification of organic compounds.
Language of instruction
Mode of study
Guarantor
Department
Learning outcomes of the course unit
1. The student will acquire techniques of organic synthesis in mines and micro scale including purification and separation techniques
2. Students will know the possibilities and limitations of individual instrumental analytical methods
3. Students will be able to interpret measured data and evaluate chemical and analytical approach in general, which will lead to considerable student independence
Prerequisites
Co-requisites
Planned learning activities and teaching methods
Assesment methods and criteria linked to learning outcomes
Course curriculum
Basic concepts, techniques and glassware, recrystallization and melting point, distillation and boiling point, extraction, methods of chromatography, spectral methods, identification of organic compounds.
1. Apparatuses for advanced organic synthesis
2. Microfiltration and its technics
3. Dry agents
4. Drying of organic solvents
5. Crystallization and crystallization technics
6. Microscale experiments
7+8. Separation technics
9. Vacuum distillation technics
10+13. NMR and interpretation
Work placements
Aims
The course structure is designed so that after completing this discipline, students are well prepared for modern research trends in the field of organic synthesis and characterization of organic molecules.
Specification of controlled education, way of implementation and compensation for absences
Recommended optional programme components
Prerequisites and corequisites
Basic literature
Recommended reading
Classification of course in study plans
- Programme DPCP_CHM_4_N Doctoral 1 year of study, winter semester, compulsory-optional
- Programme DKCP_CHM_4_N Doctoral 1 year of study, winter semester, compulsory-optional
- Programme HJR Doctoral
specialization --- , 1 year of study, winter semester, compulsory-optional