Course detail

Laboratory Classes in Analytical Chemistry II

FCH-BC_ANC2_PAcad. year: 2020/2021

Practical training at selected basic instrumental analytical methods: potentiometry, automatic titrations, spectrophotometry, fluorimetry, emission flame photometry, thin-layer chromatography, chromatography, voltammetry, electrogravimetry.

Language of instruction

Czech

Number of ECTS credits

Mode of study

Not applicable.

Guarantor

doc. Mgr. Renata Komendová, Ph.D.

Department

Institute of Chemistry and Technology of Environmental Protection (ÚCHTOŽP)

Learning outcomes of the course unit

After students finished this course, their competence inceased as follows:

1. They were practical introduced with selected analytical methods.
2. Students be able to practical aplly selected technique of determinations.
3. They practise precise work in analytical laboratory, preparation of standard solutions, good laboratory practise with samples.
4. Students will be able to use of necessary calculations and they will be used evaluation of analytical data from using analysis.

Prerequisites

Laboratory course of analytical chemistry I. Practical knowledge of basic laboratory skills: weighing, pipetting, preparation of measuring solutions, titration.
Knowledge of basic calculations used in analytical chemistry, evaluation by the calibration curve method.

Co-requisites

Not applicable.

Planned learning activities and teaching methods

The course uses teaching methods in form of Laboratory exercise - 4 teaching hours per week. The e-learning system (LMS Moodle) is available to teachers and students.

Assesment methods and criteria linked to learning outcomes

Graded course-unit credit
Requirements:
- all laboratory tasks completed, results and reports in good quality
- course test
Final classification is based on average classification of individual tasks.
Analytical results evaluation:
error to
1.5% A
3% B
5% C
7% D
9% E
error over 9% F
Overall classification:
100-90% A
89-80% B
79-70% C
69-60% D
59-50% E
49-0% F

Course curriculum

1. Introduction to practice, safety of work, methodology of work in analytical laboratory
2. Precipitation titration (Argentometry)
3. Automatic titration (alkalimetry)
4. Titration in a non-aqueous medium
5. Spectrophotometry
6. Multi-component analysis
7. Fluorimetry
8. Emission flame spectrometry
9. Voltammetry and electrogravimetry
10. Extraction spectrophotometry
11. Liquid Chromatography
12. Thin-layer chromatography

Work placements

Not applicable.

Aims

The aim of practical classes of analytical chemistry II is to learn students the base and using of selected analytical instrumental methods, such as potentiometry, automatic titration, spectrophotometry, fluorimetry, emission flame spectrometry, TLC, chromatography, voltammetry and electrogravimetry.

Specification of controlled education, way of implementation and compensation for absences

Input e-learning tests to check students' readiness.
Work in analytical laboratory.
Evaluation of analytical results.
Elaboration of the protocols.
Credit test at the end of the course.

Recommended optional programme components

Not applicable.

Prerequisites and corequisites

compulsory prerequisite
Laboratory Classes in Inorganic Chemistry I

Basic literature

Šimek Z., Komendová R., Mašek I., Voznica P. : Kvantitativní analýza. FCH VUT v Brně, Brno 2003. (CS)

Type of course unit

Laboratory exercise

52 hod., compulsory

Teacher / Lecturer

Pavla Kleinová
doc. Mgr. Renata Komendová, Ph.D.
Ing. Veronika Řezáčová, Ph.D.
Ing. Ludmila Mravcová, Ph.D.

Elearning

eLearning: currently opened course