Course detail

Instrumental and structure analysis

FCH-MC_ISAAcad. year: 2019/2020

Fundamentals, instrumentation and usage of methods of chemical, physical and structure analysis. Separation methods: chromatography methods-gas chromatography, liquid chromatography, supercritical fluid chromatography; electrophoresis, isotachophoresis. Ion mobility spectrometry. Field-flow fractionation. Thermal analysis: thermogravimetry, differential thermal analysis, differential scanning calorimetry. X-ray fluorescence spectrometry. Mass spectrometry organic and inorganic. Infrared and Raman spectrometry. Nuclear magnetic resonance spectrometry. Electron spin resonance spectrometry. Moessbauer spectrometry. Hyphenated techniques.

Language of instruction

Czech

Number of ECTS credits

Mode of study

Not applicable.

Guarantor

prof. Ing. Jiří Kučerík, Ph.D.

Department

Institute of Chemistry and Technology of Environmental Protection (ÚCHTOŽP)

Learning outcomes of the course unit

Completion of this course will increase students' competence in the following way:
a) Students will know the principles of instrumental analytical methods used in routine analytical practice
b) Students will master the methods of interpretation of the obtained measurement results both in qualitative and in quantitative terms
c) Students will be able to creatively optimize the selection of analytical techniques in solving specific analytical problem

Prerequisites

Basic knowladge of physics, general chemistry, physical chemistry, inorganic, organic, analytical chemistry and biochemistry.

Co-requisites

Not applicable.

Planned learning activities and teaching methods

The course uses teaching methods in form of Lecture - 2 teaching hours per week. The e-learning system (LMS Moodle) is available to teachers and students.

Assesment methods and criteria linked to learning outcomes

Oral examination within the range of discussed topics. Assessed is the knowledge of the principles of analytical methods including their specifics and creative ability of solution of given analytical problem.

Course curriculum

Not applicable.

Work placements

Not applicable.

Aims

The aim of this course is:
- to familiarize students with selected instrumental analytical methods used in the analytical practice
- to give them a thorough overview of the basic characteristics of these methods
- to teach students how to choose the optimal instrumental method for the concrete analytical problem

Specification of controlled education, way of implementation and compensation for absences

none

Recommended optional programme components

Not applicable.

Prerequisites and corequisites

Not applicable.

Basic literature

Kellner R., Mermet J. M., Otto M., Widmer H. M.: Analytical Chemistry. Willey-VCH, Weinheim 1998. (EN)
Sommer L.: Teoretické základy analytické chemie I., II., III. VUT Brno, Brno 1995. (CS)

Type of course unit

Lecture

26 hod., optionally

Teacher / Lecturer

Ing. Veronika Řezáčová, Ph.D.
prof. Ing. Jiří Kučerík, Ph.D.
Ing. Ludmila Mravcová, Ph.D.
doc. Mgr. Michaela Vašinová Galiová, Ph.D.
prof. Ing. Jozef Krajčovič, Ph.D.
Mgr. Helena Doležalová Weissmannová, Ph.D.