Course detail
Analytical Methods of Technical Praxis
FCH-BCO_AMPAcad. year: 2018/2019
The course content is assembled from following thematic blocks: Basic rules of analytical sampling. Procedures for sample treatments: Isolation of target analytes from sample matrix (extraction by gal, liquid, solid phase), clean-up techniques (destructive, non-destructive), methods of group separation. Instrumental analytical methods used in analytical praxis: UV-VIS spectrophotometry, separation methods (gas and liquid chromatography, electromigration techniques), mass spectrometry. Basic principles of interpretation of analytical results. Uncertainty determination.
Language of instruction
Number of ECTS credits
Mode of study
Guarantor
Learning outcomes of the course unit
1. Detailed knowledge of the complete analytical procedures used in routine analytical practice, consisting of an analytical sample collection, laboratory processing and the final analysis
2. Ability to design an optimal procedure for the analysis of a contaminant (or group of contaminants) in the environmental compartment, taking into account the specific conditions of the solved problem
Prerequisites
Co-requisites
Planned learning activities and teaching methods
Assesment methods and criteria linked to learning outcomes
Course curriculum
2. Basic principles of analytical sampling
3. Methods of target analytes isolation from sample matrix
4. Techniques of clean-up and group separation
5. UV-VIS Spectrophotometry, principle and applications
6. Gas chromatography - principle, instrumentation, application in technical praxis
7. Liquid chromatography - principle, instrumentation, application in technical praxis
8. Electromigration methods - principle, classification, instrumentation, application in technical praxis
9. Mass spectrometry - physica basics, principle, instrumentation, acquiring and interpretation of mass spectra, application for the analysis of inorganic and organic materials
10. Hyphenated techniques and their application in technical praxis
11. Basic rules of analytical results treatment and interpretation
Work placements
Aims
Specification of controlled education, way of implementation and compensation for absences
Recommended optional programme components
Prerequisites and corequisites
Basic literature
Štulík, K. a. kol.: Analytické separační metody. 1. vyd. Praha: KU Praha, 2005 (CS)
Volka, K. a. kol.: Analytická chemie 2. 1. vyd. Praha: Vydavatelství VŠCHT, 1995 (CS)
Recommended reading
Classification of course in study plans
- Programme BKCP_CHCHT Bachelor's
branch BKCO_CHTOZP , 3 year of study, winter semester, compulsory
- Programme BPCP_CHCHT Bachelor's
branch BPCO_CHTOZP , 3 year of study, winter semester, compulsory
- Programme CKCP_CZV lifelong learning
branch CKCO_CZV , 1 year of study, winter semester, compulsory