Course detail
Laboratory Classes in Instrumental and Structure Analysis - MS
FCH-MCA_ISA_MAcad. year: 2012/2013
Students are introduced with basic methods making possible uncovering, observation and evaluation of supramolecular structure of polymer materials both theoretically and practically. Microscopy, spectroscopy and thermal methods are used. The half of the subject time serves to obtain theoretical background of selected methods and the other one to practice them. The stress is laid on proper preparation of the sample, suitable setting of testing conditions, accurate evaluation and interpretation of obtained data including examination of the method availability for tested material.
Language of instruction
Number of ECTS credits
Mode of study
Guarantor
Department
Learning outcomes of the course unit
Prerequisites
Co-requisites
Planned learning activities and teaching methods
Assesment methods and criteria linked to learning outcomes
- the attendance in all theoretical and laboratory practics,
- producing and handover of all laboratory reports in time and in demanded quality,
- passing thematic tests
- passing the credit test – minimum score is 50%
Course curriculum
Theory: Morphology of polymers, optical microskopy (OM); test from morphology and OM
Practice: Isothermal crystallization of thermoplastics using OM and evaluation of sperulites morphology
Theory: Methods for uncovering supramolecular structure of thermoplastics; Confocal laser scanning microscopy (CLSM); test from methods used for uncovering of supramolecular structure and CLSM
Practice: Chemical etching of thermoplastics and observation of the etched surfaces on CLSM
Theory: Differential scanning calorimetry (DSC); test from DSC
Practice: DSC of polymers
Theory: Fourier Transform Infrared spectroscopy (FTIR); test from FZIR
Practice: FTIR analysis of polymers and fillers
Credit test
Work placements
Aims
Specification of controlled education, way of implementation and compensation for absences
Theoretical knowledge of students regarding the particular theme is examined by written tests.
Laboratory reports are handover according the instructions of lecturer.
Recommended optional programme components
Prerequisites and corequisites
Basic literature
EHRENSTEIN, GW. Polymeric Materials : Structure – Properties – Applications. Munich : Carl Hanser Verlag, 2001. 279 p. ISBN 3-446-21461-5. (CS)
LEDNICKÝ, František. Mikroskopie a morfologie polymerů : Díl 1. Mikroskopie polymerů a preparační techniky. 1. vyd. Liberec : Fastr typo-tisk, 2009. 71 s. ISBN 978-80-7372-486-3. (CS)
LEDNICKÝ, František. Mikroskopie a morfologie polymerů : Díl 2. Morfologie polymerů. 1. vyd. Liberec : Fastr typo-tisk, 2009. 97 s. ISBN 978-80-7372-486-3.3. (CS)
Recommended reading
Classification of course in study plans
Type of course unit
Guided consultation in combined form of studies
Teacher / Lecturer
Laboratory exercise
Teacher / Lecturer