Course detail

Laboratory Classes in Analytical Chemistry II

FCH-BCA_ANC2_PAcad. year: 2012/2013

Practical training at selected basic instrumental analytical methods: potentiometry, automatic titrations, spectrophotometry, fluorimetry, emission flame photometry, thin-layer chromatography, ionex chromatography, electrogravimetry.

Language of instruction

Czech

Number of ECTS credits

Mode of study

Not applicable.

Guarantor

doc. Mgr. Renata Komendová, Ph.D.

Department

Institute of Chemistry and Technology of Environmental Protection (ÚCHTOŽP)

Learning outcomes of the course unit

After student finished this course, he was practical introduced with selected analytical procedures and methods, with evaluation of results, obtaining skills essential for experimentation, sample handling according to GLP and with practising of calculations used in analytical chemistry too.

Prerequisites

Laboratory course of analytical chemistry I.

Co-requisites

Not applicable.

Planned learning activities and teaching methods

Teaching methods depend on the type of course unit as specified in the article 7 of BUT Rules for Studies and Examinations.

Assesment methods and criteria linked to learning outcomes

Graded course-unit credit
Requirements:
- all laboratory tasks completed, results and reports in good quality
- course test
Final classification is based on average classification of individual tasks.

Course curriculum

Introduction, work safety, analytical laboratory techniques
Redox and potentiometric titrations
Potentiometric titrations (precipitation titrations)
Automatic acid-base titrations
Titrations in nonaqueous solvents
Spectrophotometry
Spectrophotometry in mixtures
Extraction spectrophotometry
Fluorimetry
Emission flame spectrometry
Chromatographic methods (TLC, IEC)
Analysis of copper-based alloys

Work placements

Not applicable.

Aims

Familiarization of students with the basic instrumental methods used in analytical chemistry, such as potentiometry, automatic titration, spectrophotometry, fluorimetry, emission flame spectrometry, TLC, chromatography and electrogravimetry.

Specification of controlled education, way of implementation and compensation for absences

Written entrance tests at the beginning of all exercises checking the students readiness for practical work.
Elaboration of the protocols on a given exercises.
Credit test at the course end.

Recommended optional programme components

Not applicable.

Prerequisites and corequisites

Not applicable.

Basic literature

Komendová R., Praktikum z analytické chemie II, BCA_ANC2_P, https://www.vutbr.cz/elearning/ (CS)
Šimek Z., Komendová R., Mašek I., Voznica P. : Kvantitativní analýza. FCH VUT v Brně, Brno 2003. (CS)

Type of course unit

Laboratory exercise

65 hod., compulsory

Teacher / Lecturer

Jitka Pochopová
Ing. Veronika Řezáčová, Ph.D.
Ing. Josef Kotlík, CSc.
doc. Mgr. Renata Komendová, Ph.D.
Ing. Ludmila Damborská
RNDr. Jaroslav Mega, Ph.D.