Course detail
Analytical Chemistry II
FCH-BCA_ANC2Acad. year: 2012/2013
This course aims to introductuion students to the basic methods and techniques of instrumental analytical chemistry. Teaching is structured in the following thematic areas:Physical aspects of analytical methods. Analytical signal and its qulitative and quantitative evaluation. Principles of selected instrumental methods-spectrometric and electroanalytical methods, their qualitative and quantitative aspects and practical examples. Principles of selected separation methods, principles of chromatographic and electromigration methods. Evaluation of analytical results. Basics of chemometry. Preparation and decomposition of inorganic, organic and biological samples for analysis.
Language of instruction
Number of ECTS credits
Mode of study
Guarantor
Learning outcomes of the course unit
1. They will know in depth the principles of simple instrumental analytical methods and possibilities of their application.
2. They will be able to select the optimal method for solving of specific analytical problems of analytical practice.
3. They will adopt the basic principles of chemometrictreatment of analytical results obtained using simple instrumental-analytical methods.
Prerequisites
Co-requisites
Planned learning activities and teaching methods
Assesment methods and criteria linked to learning outcomes
Condition for passing the exam is a credit from the exercise of Analytical Chemistry II.
The exam is oral, the degree of knowledge of the fundamentals of theory and practice of analytical chemistry and creative approach in solving analytical problems is assessed.
Course curriculum
Potentiometry
Voltammetry, polarography (classic, differential pulse, dissolition, adsorptive)
Potentiometric dissolution analysis, titrations with polarizable electrodes¨
Electrogravimetry, coulometry, conductometry.
Block 2: Optical methods
Classification of spectral methods, basic physical principles, properties of electromagnetic radiation
Non-spectral methods: Refractometry, interferometry, polarimetry, nephelometry, turbidimetry
Spectral methods: UV-VIS spectrophotometry - principles, properties, construction of spectrophotometers, applications
Luminescence methods: molecular fluorescence, phosphorescence, chemiluminiscence, bioluminiscence and their analytical applications
Basics of otical atomic spectrometry
Block 3: Principles and applications of basic chromatographic and electromigration techniques
Basic principles of chromatography, separation mechanisms
Chromatographic techniques - paper chromtaography, thin-layer chromatography, column chromatography
Basics of modern liquid and gas chromatography
Separation in electric field - principles, application (electrophoresis)
Work placements
Aims
Specification of controlled education, way of implementation and compensation for absences
Consultations for students in distant form.
Consultations for regular students.
Recommended optional programme components
Prerequisites and corequisites
Basic literature
Sommer L.: Základy analytické chemie II. VUTIUM, Brno 1998. (CS)
Volka K.: Analytická chemie II. VŠCHT Praha, 1997. (CS)
Recommended reading
Classification of course in study plans
- Programme BPCP_CHCHT Bachelor's
branch BPCO_CHM , 2 year of study, summer semester, compulsory
branch BPCO_CHTOZP , 2 year of study, summer semester, compulsory
branch BPCO_SCH , 2 year of study, summer semester, compulsory - Programme BKCP_CHCHT Bachelor's
branch BKCO_SCH , 2 year of study, summer semester, compulsory
branch BKCO_CHTOZP , 2 year of study, summer semester, compulsory
branch BKCO_CHM , 2 year of study, summer semester, compulsory - Programme BKCP_CHTP Bachelor's
branch BKCO_PCH , 2 year of study, summer semester, compulsory
branch BKCO_BT , 2 year of study, summer semester, compulsory - Programme BPCP_CHTP Bachelor's
branch BPCO_BT , 2 year of study, summer semester, compulsory
branch BPCO_CHP , 2 year of study, summer semester, compulsory - Programme BPCP_CHCHT Bachelor's
branch BPCO_CHMN , 2 year of study, summer semester, compulsory
branch BPCO_CHTOZP , 2 year of study, summer semester, compulsory - Programme CKCP_CZV lifelong learning
branch CKCO_CZV , 1 year of study, summer semester, compulsory
- Programme BPCP_CHCHT_AKR Bachelor's
branch BPCO_CHM , 2 year of study, summer semester, compulsory
branch BPCO_CHTOZP , 2 year of study, summer semester, compulsory
branch BPCO_SCH , 2 year of study, summer semester, compulsory
Type of course unit
Guided consultation in combined form of studies
Teacher / Lecturer
Exercise
Teacher / Lecturer