Publication detail

Mapping of different structures on large area of garnite sample using laser-ablation based analytical techniques, an exploratory study

NOVOTNÝ, Karel - KAISER, Jozef - GALIOVÁ, Michaela - KONEČNÁ, Veronika - NOVOTNÝ, Jan - MALINA, Radomír - LIŠKA, Miroslav - KANICKÝ, Viktor - OTRUBA, Vítězslav

Original Title

Mapping of different structures on large area of garnite sample using laser-ablation based analytical techniques, an exploratory study

Type

journal article - other

Language

English

Original Abstract

Laser-ablation based analytical techniques represent a simple way for fast chemical analysis of different materials. In this work, an exploratory study of multi-element (Ca, Al, Fe, Mn) mappings of a granite sample surface was performed by laser induced breakdown spectroscopy (LIBS) and subsequently by laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) analysis. The operating parameters (e.g. pulse energy, ablation-crater size) were optimized for both techniques in order to achieve the appropriate conditions for two-dimensional high-resolution compositional mappings of mineral microstructures in large sample areas. The sample was scanned with 100 x 100 individual sample points to map an area of 20 x 20 mm2. The normalized signals were used for construct of contour plots which were colored according local distribution of the selected elements. The results of two laser-based methods were compared and found to be similar.

Keywords

LIBS; LA-ICP-MS; Geological samples; Spatially-resolved analysis; Compositional mapping

Authors

NOVOTNÝ, Karel - KAISER, Jozef - GALIOVÁ, Michaela - KONEČNÁ, Veronika - NOVOTNÝ, Jan - MALINA, Radomír - LIŠKA, Miroslav - KANICKÝ, Viktor - OTRUBA, Vítězslav

RIV year

2008

Released

1. 10. 2008

Publisher

Elsevier Science

Location

Amsterdam, Nizozemsko

ISBN

0584-8547

Periodical

Spectrochimica Acta Part B

Year of study

62B

Number

10

State

United Kingdom of Great Britain and Northern Ireland

Pages from

1139

Pages to

1144

Pages count

6

BibTex

@article{BUT47346,
  author="Jozef {Kaiser} and Michaela {Vašinová Galiová} and Jan {Novotný} and Radomír {Malina} and Miroslav {Liška}",
  title="Mapping of different structures on large area of garnite sample using laser-ablation based analytical techniques, an exploratory study",
  journal="Spectrochimica Acta Part B",
  year="2008",
  volume="62B",
  number="10",
  pages="1139--1144",
  issn="0584-8547"
}