Publication detail

Correlation of Acoustic and Optical Emission Signals Produced at 1064 and 532 nm Laser-induced Breakdown Spectroscopy (LIBS) of Glazed Wall Tiles

HRDLIČKA, A. -ZAORÁLKOVÁ, L. -GALIOVÁ, M. -ČTVRTNÍČKOVÁ, T. -KANICKÝ, V. -OTRUBA, V. -NOVOTNÝ, K. -KRÁSENSKÝ, P. -KAISER, J. -MALINA, R. -PÁLENÍKOVÁ, K.

Original Title

Type

journal article - other

Language

English

Original Abstract

An acoustic signal was used for the internal standardization of laser-induced breakdown spectroscopy (LIBS) of a glazed wall tile. For the LIBS analyses, 1064 nm and 532 nm wavelengths of the Nd:YAG laser were utilized. The tile was depth profiled by a single-spot ablation from the glaze into the substrate. Some lines of major elements Si(I) 252.418, Si(I) 252.851, Al(I) 257.509, Cr(I) 295.368, Al(I) 309.271 nm and Ti(II) 334.904 nm were monitored. The decrease in the optical emissions during the ablation was successfully compensated for by normalization to the square power of the acoustic signal in the interval of 290-340 nm. This approach failed for the lines between 250-270 nm. The results were the same for both lasing wavelengths despite different irradiances. The acquired profiles are in good agreement with the reference X-ray fluorescence measurement.

Keywords

LIBS, Acoustic signal, Normalization, Internal standard, Ceramic tile, Depth profiling

Authors

HRDLIČKA, A. -ZAORÁLKOVÁ, L. -GALIOVÁ, M. -ČTVRTNÍČKOVÁ, T. -KANICKÝ, V. -OTRUBA, V. -NOVOTNÝ, K. -KRÁSENSKÝ, P. -KAISER, J. -MALINA, R. -PÁLENÍKOVÁ, K.

RIV year

2008

Released

24. 10. 2008

ISBN

0584-8547

Periodical

Spectrochimica Acta Part B

Year of study

Number

State

United Kingdom of Great Britain and Northern Ireland

Pages from

Pages to

Pages count

BibTex

@article{BUT48350,
  author="Jozef {Kaiser} and Radomír {Malina} and Kateřina {Brillová}",
  title="Correlation of Acoustic and Optical Emission Signals Produced at 1064 and 532 nm Laser-induced Breakdown Spectroscopy (LIBS) of Glazed Wall Tiles",
  journal="Spectrochimica Acta Part B",
  year="2008",
  volume="64",
  number="1",
  pages="74--78",
  issn="0584-8547"
}