Detail publikace
Method optimization for analysis of aroma compounds of cheeses by SPME
VÍTOVÁ, E. MIKULÍKOVÁ, R. DRDÁK, M. BŘEZINA, P.
Originální název
Method optimization for analysis of aroma compounds of cheeses by SPME
Typ
článek v časopise - ostatní, Jost
Jazyk
angličtina
Originální abstrakt
Three different isolation techniques were tested for the study of mould cheeses aroma compounds: steam distillation, headspace and solid phase microextraction. SPME was chosen and optimised as the most convenient. It offers many advantages: simplicity, rapidity and first of all minimizing thermal, chemical and mechanical modifications of the sample. The volatile components were extracted using CarboxenTM/Polydimethylsiloxane fiber and analysed by gas chromatography. The method showed good reproducibility and sensitivity. Linearity was excellent ( R2 0.9564-0.9952). 46 compounds were identified in Niva cheese using this method: 3 hydrocarbons, 2 aldehydes, 9 ketones, 16 alcohols, 2 esters, 10 fatty acids and 1 sulphur compound. Present contaminants (silicone, phthalates) come probably from laboratory material used.
Klíčová slova
cheese, SPME, aroma
Autoři
VÍTOVÁ, E.; MIKULÍKOVÁ, R.; DRDÁK, M.; BŘEZINA, P.
Rok RIV
2003
Vydáno
1. 1. 2002
Nakladatel
ČSCH
Místo
Brno
ISSN
0009-2770
Periodikum
Chemické listy
Ročník
96
Číslo
6
Stát
Česká republika
Strany od
497
Strany do
498
Strany počet
1
BibTex
@article{BUT41219,
author="Eva {Vítová} and Renata {Mikulíková} and Milan {Drdák} and Pavel {Březina}",
title="Method optimization for analysis of aroma compounds of cheeses by SPME",
journal="Chemické listy",
year="2002",
volume="96",
number="6",
pages="497--498",
issn="0009-2770"
}