Detail předmětu
Instrumental and Structural Analysis
FCH-MA_ISAAk. rok: 2024/2025
The students will be acquainted with theoretical fundamentals and application of methods of chemical, physical and structural analysis. The course also includes advanced separation and electromigration techniques, organic Mass Spectrometry with emphasis on tandem techniques, Infrared and Raman Spectroscopy, Thermogravimetry, Differential Thermal Analysis, Differential Scanning Calorimetry, X-Ray Fluorescence, X-Ray Diffraction, Auger Electron Spectroscopy, Nuclear Magnetic Resonance and Electron Microscopy. The overview is completed with inorganic analysis techniques, such as Atomic Absorption Spectrometry, Emission and Fluorescence Spectrometry together with Inductively Coupled Plasma Mass Spectrometry and Inductively Coupled Plasma Optical Emission Spectrometry.
Jazyk výuky
Počet kreditů
Garant předmětu
Nabízen zahraničním studentům
Pravidla hodnocení a ukončení předmětu
Written examination including all topics discussed. If more than 50% are obtained, an oral exam follows. The knowledge of principles of analytical methods including their particularities, and ability of creative solution of analytical problems are evaluated. Final evaluation corresponds to ECTS system.
Attendance at the lecture is not required, but recommended.
Učební cíle
Základní literatura
Crouch S. a Skoog D., Principles of Instrumental Analysis, Cengage Learning, Inc., 2017. (EN)
Skoog D. A., West D. M., Holler F. J., Crouch S. R.: Fundamentals of Analytical Chemistry, Cengage Learning, Inc., 2014. (EN)
Zařazení předmětu ve studijních plánech
- Program NKCP_CHPL magisterský navazující 1 ročník, zimní semestr, povinný
- Program NPCP_CHPL magisterský navazující 1 ročník, zimní semestr, povinný
- Program NPCP_ECHT magisterský navazující 1 ročník, zimní semestr, povinný
- Program NKCP_ECHT magisterský navazující 1 ročník, zimní semestr, povinný
- Program NPAP_ENVI magisterský navazující 1 ročník, zimní semestr, povinný
Typ (způsob) výuky
Přednáška
Vyučující / Lektor
Osnova
The students will be acquainted with theoretical fundamentals and application of methods of chemical, physical and structural analysis. The course also includes advanced separation and electromigration techniques, organic Mass Spectrometry with emphasis on tandem techniques, Infrared and Raman Spectroscopy, Thermogravimetry, Differential Thermal Analysis, Differential Scanning Calorimetry, X-Ray Fluorescence, X-Ray Diffraction, Auger Electron Spectroscopy, Nuclear Magnetic Resonance and Electron Microscopy. The overview is completed with inorganic analysis techniques, such as Atomic Absorption Spectrometry, Emission and Fluorescence Spectrometry together with Inductively Coupled Plasma Mass Spectrometry and Inductively Coupled Plasma Optical Emission Spectrometry.
1. Advanced separation techniques
2. Electromigration methods
3. Organic Mass Spectrometry
4. Infrared Spectroscopy, Raman Spectroscopy
5. Atomic Absorption Spectrometry
6. Atomic Emission Spectrometry (AES, AFS), Inductively Coupled Plasma spectrometry
7. Inductively Coupled Plasma Mass Spectrometry, Inductively Coupled Plasma Optical Emission Spectrometry
8. Thermal Analysis – Thermogravimetry, simultaneous methods
9. Thermal Analysis – Differential Thermal Analysis, Differential Scanning Calorimetry
10. X-Ray Fluorescence, Auger Electron Spectroscopy
11. Electron Microscopy
12. X-Ray Diffraction
13. Nuclear Magnetic Resonance
Konzultace v kombinovaném studiu
Vyučující / Lektor